Webrate of 100°C/min. Initially the set point for furnace control begins heating at 100°C/min. The furnace lags behind the set point temperature; the surface that supports the sample pan lags behind the furnace, the sample pan lags behind the DSC cell, and there are even temperature gradients across the sample specimen itself. Differential scanning calorimetry (DSC) is a thermoanalytical technique in which the difference in the amount of heat required to increase the temperature of a sample and reference is measured as a function of temperature. Both the sample and reference are maintained at nearly the same temperature throughout the experiment. Generally, the temperature program for a DSC an…
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